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Table 2 Chemical shifts (δ13C/δ1H) (ppm) of polysaccharide components assigned in this study (DMSO-d 6 and pyridine-d 5 = 4:1)

From: Precipitate obtained following membrane separation of hydrothermally pretreated rice straw liquid revealed by 2D NMR to have high lignin content

 

1

2

3

5

(1,4)-β-D-Glcp

103.2/4.57, 103.3/4.36

   

(1,4)-β-D-Glcp(R)

97.2/4.58

   

(1,4)-α-D-Glcp(R)

92.7/5.17

   

2-O-Ac-β-D-Xylp

99.7/4.68

73.8/4.74

  

3-O-Ac-β-D-Xylp

101.9/4.62

 

75.3/5.03

 

(1,4)-β-D-Xylp

102.0/4.46

  

63.5/3.46, 63.4/4.15, 63.7/4.07, 63.3/3.35

(1,4)-β-D-Xylp(R)

98.0/4.48

   

(1,4)-α-D-Xylp(R)

92.8/5.08

   

α-L-Araf

107.8/5.63

   

α-L-Fucp

100.6/5.34, 101.1/5.26

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