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Table 3 Proportion of different crystalline cellulose and the CrI of cellulose

From: Precise pretreatment of lignocellulose: relating substrate modification with subsequent hydrolysis and fermentation to products and by-products

Crystalline types

Chemical shift (ppm)

Proportion (%)

S

DS

PS2

PS3

NS

Cellulose I (C6)

64.5–66.0

28.1

36.9

27.4

32.0

7.91

Cellulose II (C1)

106.0–107.0

NDa

NDa

NDa

NDa

11.8

Cellulose I α (C1)

104.9 (0.1)

62.5

59.6

43.7

35.1

8.90

Cellulose I β (C1)

105.9, 103.8

15.8

26.8

32.2

51.9

49.5

Less-ordered (C1)

103.2, 102.6 (0.2) 21.7

21.7

13.6

24.1

13.0

27.8

Crystallinity index CrI

35.4

45.8

32.8

29.6

16.8

  1. a ND Not detected