PS | PS-Air | PS-N2 | |||||
---|---|---|---|---|---|---|---|
6% | 9% | 12% | 6% | 9% | 12% | ||
XRD | |||||||
CrI % | 64.4 | 49.9 | 47.5 | 44.4 | 59.3 | 62.6 | 60.3 |
2θ IAM (°) | 18.92 | 19.18 | 19.12 | 18.85 | 18.96 | 18.99 | 18.73 |
IAM (CPS) | 2.42 | 4.56 | 2.99 | 8.18 | 2.99 | 2.48 | 7.83 |
2θ I200 (°) | 22.57 | 22.57 | 22.57 | 22.63 | 22.58 | 22.57 | 19.72 |
I200 (CPS) | 6.81 | 9.09 | 5.70 | 14.7 | 7.51 | 6.63 | 22.66 |
13C NMRb | |||||||
Int.(89) | 1307 | 961 | 865 | 865 | 1172 | 1145 | 1114 |
Int.(84) | 716 | 544 | 497 | 496 | 626 | 626 | 606 |
Int.(89)/Int.(84) | 1.83 | 1.77 | 1.74 | 1.74 | 1.85 | 1.83 | 1.84 |
CrI (%) | 64.6 | 63.9 | 63.5 | 63.6 | 64.9 | 64.7 | 64.8 |