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Table 1 Composition of pretreated solids at different pretreatment conditions

From: A novel hybrid organosolv: steam explosion method for the efficient fractionation and pretreatment of birch biomass

Pretreatment conditions

Biomass solubilization (% of initial biomass)

Cellulose (% w/w)

Hemicellulose (% w/w)

Lignin (% w/w)

Ethanol effect

30 min

50% v/v

47.9

65.9 (1.2%)

15.1 (74.8%)

6.7 (81.2%)

60% v/v

48.9

67.1 (1.3%)

21.0 (65.7%)

7.1 (80.5%)

70% v/v

41.5

61.7 (0.0%)

21.9 (59.0%)

8.7 (72.6%)

Time effect

60% v/v

15 min

44.7

66.3 (0.0%)

22.0 (61.1%)

7.8 (77.0%)

30 min

48.9

67.1 (1.3%)

21.0 (65.7%)

7.1 (80.5%)

60 min

40.0

60.7 (0.0%)

19.1 (63.4%)

13.2 (57.5%)

Catalyst effect

15 min—60% v/v ethanol

0%

44.7

66.3 (0.0%)

22.0 (61.1%)

7.8 (77.0%)

0.2%

45.0

61.1 (3.2%)

25.8 (54.5%)

7.4 (78.2%)

1%

63.1

77.9 (17.2%)

8.9 (89.5%)

7.0 (86.2%)

  1. All results are expressed based on dry mass. Numbers in parenthesis represent the mass fraction of each component (i.e., cellulose, hemicellulose, and lignin) that was solubilized at the end of the pretreatment (calculated using Eq. 1). Compositional analysis was performed in duplicates, and the standard error was > 5% of the value. All the trials were done with the explosive discharge step at the end of the treatment