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Table 3 XPS, acetyl, hydrophobicity, and crystallinity index (%) analysis of non-pretreated and 5% AC-pretreated poplar

From: Production of xylooligosaccharides and monosaccharides from poplar by a two-step acetic acid and peroxide/acetic acid pretreatment

Treatment time

C1 (%)

C2 (%)

C3 (%)

O/C

Acetyl (%)

Hydrophobicity (L/g)

Crystallinity index (%)

Raw poplar

54.0

35.8

10.2

0.68

3.7 ± 0.2

0.37

47.1

10 min

56.0

34.0

10.0

0.37

5.7 ± 0.0

0.54

48.9

30 min

53.8

37.9

8.3

0.40

5.9 ± 0.0

0.49

55.2

50 min

49.4

44.5

6.1

0.41

5.7 ± 0.2

0.31

56.7

  1. C1 corresponds to class of carbon that corresponds to carbon atoms bonded to carbon or hydrogen (C–C)
  2. C2 corresponds to class of carbon atoms bonded to single non-carbonyl oxygen (C–O)
  3. C3 corresponds to class of carbon atoms bonded to a carbonyl or two non-carbonyls (C=O or O–C–O)