Table 2 Structure determination and refinement statistics. Values in parentheses are for the outermost shell
PDB code | 8C10 |
Resolution range (Å) | 45.04–1.00 (1.02–1.00) |
Completeness (%) | 97.85 (79.7) |
s cutoff | None |
No. of reflection, working set | 140,934 |
No. of reflection, reference set | 2221 |
Final Rwork | 11.42 |
Final Rfree | 13.39 |
Cruickshank DPI | 0.0178 |
No. of non-H atoms | |
Protein | 2427 |
Water | 339 |
Other* | 19 |
Total | 2785 |
R.m.s. deviations | |
Bonds (Å) | 0.0291 |
Angles (°) | 2.31 |
Average B factors (Å2) | |
Overall | 11.37 |
Protein | 9.71 |
Water | 22.75 |
Other* | 20.70 |
Ramachandran plot (%) | |
Preferred | 96.61 |
Allowed | 3.39 |
Outliers | 0 |